Effects of incorporating magnesium oxide and zirconium dioxide nanoparticles in acrylic resin denture base material: a comparative study
AuthorsZena J. Wally, Ola M. Al-Jubouri, Zaid G. Al-Jlaihawi, Rajaa M. Almusawi, Rasha A. Alamoush and Julfikar Haiderr
JournalFrontiers in Dental Medicine
Date2025-10-07
AbstractThe current study aimed to evaluate the effects of incorporating
magnesium oxide (MgO) and zirconium oxide (ZrO2) nanoparticles individually or
in combination into heat-cured acrylic resin on the polymer structure, density,
surface roughness, hardness and flexural strength for denture base applications.
MgO and ZrO2 nanoparticles strengthen the polymer matrix by
forming coordination bonds with carbonyl oxygens, increasing crosslinking. This
increased the density and flexural strength while reducing the surface roughness
but lowered the hardness at elevated concentrations. These findings suggest the
potential for tailored polymer applications, improved denture performance,
increased patient comfort, and longer-lasting dental prostheses.
The effect of using modified Flask on some properties of Heat-Cure Acrylic Resin
AuthorsAli M. alqurashi, Sadiq A. almayali, Ola M. Al-Jubouri, Rajaa. M. Almusawi, Zena J. Wally, Hussein J. Abd Noor, Batool M. Fahham
JournalAIN SHAMS DENTAL JOURNAL
Date2025-06-01
AbstractThe paper aimed to evaluate using a modified flask on surface hardness and roughness, flexural, and tensile strength for
heat-polymerized acrylic resin.
According to the result of this study, the mechanical properties of heat-polymerized acrylic resin were improved
using a modified flask with a new metal plate.
The Effects of Incorporating Ag-Zn Zeolite on the Surface Roughness and Hardness of Heat and Cold Cure Acrylic Resins
AuthorsAli M. Aljafery, Ola M. Al-Jubouri , Zena J.Wally , Rajaa M. Almusawi , Noor H. Abdulrudha and Julfikar Haider
JournalJournal of Composites Science
Date2022-03-09
AbstractOne of the most widely used materials for the fabrication of prosthetic dental parts is
acrylic resin. Its reasonable mechanical and physical properties make it a popular material for a wide
range of dental applications. Recently, many attempts have been made to improve the mechanical
and biological properties of this material, such as by adding fibres, nanoparticles, and nanotubes.
The current study aimed to evaluate the effects of adding an antimicrobial agent, Ag-Zn zeolite,
on the surface roughness and hardness of the denture base resins. Ag-Zn zeolite particles were
chemically prepared and added at different concentrations (0.50 wt.% and 0.75 wt.%) to the heat cure
(HC) and cold cure (CC) acrylic resins. Zeolite particles were characterized and confirmed using
X-ray diffraction (XRD) and Energy-Dispersive X-ray Spectroscopy (EDX) attached with a Scanning
Electron Microscope (SEM). Sixty disk shape specimens (40 mm diameter and 2 mm thickness) were
fabricated from the HC and CC resins with and without the zeolite. All the specimens were divided
into two main groups based on the acrylic resins, then each was subdivided into three groups (n = 10)
according to the concentration of the Ag-Zn zeolite. A surface roughness and a hardness tester were
used to measure the surface finish and hardness of the specimens. The analysed data showed that
the surface roughness values significantly decreased when 0.50 wt.% and 0.75 wt.% zeolite were
incorporated in the HC resin specimens compared to the control group. However, this reduction
was not significant in the case of CC resin, while the surface hardness was significantly improved
after incorporating 0.50 wt.% and 0.75 wt.% zeolite for both the CC and HC resins. Incorporating
Ag-Zn zeolite with acrylic resin materials could be beneficial for improving their surface finish and
resistance to surface damage as defined by the higher hardness.
Evaluation the Linear Dimensional Changes and Hardness of Gypsum Product / Stone Type IV after Adding Silica Nanoparticles
AuthorsOla Mohammed Aljubori, Ali Mohammad Ali Aljafery , Raja'a Mahdi Al-Mussawi
JournalNano Biomedicine and Engineering
Date2020-08-11
Abstractwith some acceptable linear dimensional changes in the finished restorations. This study aimed to
evaluate linear dimensional stability and surface hardness of dental stone type IV when adding silica
nanoparticles to it. 40 type IV stone specimens were prepared from stainless steel molds for linear
dimensional stability and plastic mold for hardness, 20 of which contained silica nanoparticles (test
group) while the other 20 were without any addition (control group). Each group was divided into
subgroups containing 10 specimens for each one in order to compare the dimensional stability and
hardness of them. The linear dimensional changes were measured using a digital caliper, while the
hardness was tested with Vickers’ hardness test. The data were analyzed with t-test (two-sample
assuming unequal variances) and p-value. The mean value of linear dimensional changes for the
control group was -0.396 and -0.386 for specimens of the test group. Mean hardness was 50.638 for
the control group and 53.295 for the test group. The difference was significant for linear dimensional
changes and highly significant for hardness. Adding of silica nanoparticles improved the hardness and
reduced the linear dimensional changes of type IV stone.
Sudying the effect of adding Titanium Dioxide (TiO2) nanoparticles on the compressive strength of chemical and heat-activated acrylic denture base resins
AuthorsWasnaa M. Abdulridha, Rajaa M. Almusawi , Ola M. Al-Jubouri , Zena J. Wally , Saleh Zidan , Julfikar Haider & Nibrass T. Al-Quraine
JournalAdvances in Materials and Processing Technologies
Date2020-10-29
AbstractThe commonly used acrylic resins for fabricating denture base suffer
from poor mechanical properties. This study aimed to assess the effect
of incorporating Titanium Dioxide (TiO2) nanoparticles (NPs) as
a reinforcement agent on the compressive strength of different acrylic
denture base materials. Thirty-two cylindrical specimens (22 mm in
height and 12 mm in diameter) were prepared from PMMA resins with
and without TiO2 NPs. They were allocated into two main groups
according to the materials used such as cold cure and heat cure
denture base resins and then divided into two subgroups each containing
eight specimens: control (without nanoparticles) and experimental
(with 2 wt.% TiO2 NPs). TiO2 NPs were synthesised via a chemical
processing route. Particle morphology and size distribution were
assessed using SEM and AFM while XRD technique was employed to
determine the crystalline structure of the NPs. Compression test was
performed on the specimens using a universal Instron testing machine
to compare the compressive strength. Size of crystalline TiO2 NPs varied
between 40 and 80 nm. The mean compressive strength for the cold
cure acrylic resin (control group) and its nanocomposite (experimental
group) were found to be 15.37 MPa and 17.42 MPa while for the heat
cure acrylic resin and its nanocomposite were 23.04 MPa and 24.30
MPa. A statistically significant difference was recorded between the
compressive strengths of cold cure acrylic resin and its nanocomposite.
However, the difference was non-significant in the case of heat cure
acrylic resin. The compressive strengths of both cold cure and heat cure
acrylic resins increased after the incorporation TiO2 NPs.