A Green Product Using Selective Compound for Susceptible Assessment of Copper in Blood Serum
الباحث الأول:
Hussain Kirem
الباحثين الآخرين:
Naser Abdulhasan Naser
المجلة:
Current Applied Science and Technology
تاريخ النشر:
None
مختصر البحث:
A highly reliable approach for assessenent of copper(11) in blood serum samples using an organic molecule 4-43-hydroxyphenylazo)resorcinol, 4-HAR was developed. The paper presents the synthesis of 4-HAR which serves as probe for definite species. 4-…
A highly reliable approach for assessenent of copper(11) in blood serum samples using an organic molecule 4-43-hydroxyphenylazo)resorcinol, 4-HAR was developed. The paper presents the synthesis of 4-HAR which serves as probe for definite species. 4-HAR was characterized with the FT-IR, UV-visible, H-NMR. C-NMR and miss analysis, thermal TG and DSC techniques. After examining its interachons with more than twenty-five metal ions, it was found that 4-HAR showed reaction only with copperill), giving a distinct green color at Amax 603 nm. Experimental conditions for the reaction of 4-HAR with copper(II) were optimized A calibration curve was created and the exhibition range of concentration obeyed Beer's Law from 10.30 to 16 µg ml. with correlation coefficient ofr-0.9986, and value of the molar absorption coefficient, s, being 3314 Lmol cm. The analytical method was used to determine copper(II) levels in several hlood serum samples. The ankrunts of copper(11) found in the sera samples were compared with flame atomic absorption spectrometry technique, and the results were found to be highly reliable, Based on validation, the new approach can be utilized for assurance quality purposes with a high degree of confidence
