الخلاصة
The research includes preparation and identification of new aza reagent
2-{(6-mthyl benzothiazol azo) -1- naphthol -4-sulfonic} by infrared
(FTIR), spectrophotometric Uv- vis, melting point. This reagent used
for estimation copper (II) in new design of (FIA) system, the various
parameters (chemical and physical) affecting on estimation have been
investigated such as flow rate was 9 ml/min, reaction coil 35 cm,
volume reagent 335.5 μl, volume sample 196.25. μl, pH was 7 and
reagent concentration 10-4 M, after that preparation the calibration
curve in flow injection analysis system, the average desperation
coefficient was 1.117 and reliability were studied. Compared between two methods
(spectrophotometric method and FIA method).
KEYWORD: Copper ion, Determination, Flow Injection |