Benner
عباس محمد العباسي ( مدرس )
كلية الصيدلة
[email protected]
009647814470013
 
 
 
Influence of deposition temperature on the growth of rutile TiO2 nanostructures by CBD method on seed layer prepared by RF magnetron sputtering
تحميل
بحث النوع:
علوم التخصص العام:
Abbas M. Selman اسم الناشر:
Z. Hassan اسماء المساعدين:
Journal of Superlattices and Microstructures -ELSEVIER: Impact Factor: 2.1- الجهة الناشرة:
, Superlattices and Microstructures, 64 (2013) 27–36. (ELSEVIER: Impact Factor: 2.1)  
2013 سنة النشر:

الخلاصة

Rutile titanium dioxide (TiO2) nanostructures were successfully fabricated using the simple chemical bath deposition method at various deposition temperatures. These nanostructures were fabricated on (100 ± 10 nm) TiO2 seed layer coated glass, which was prepared via radio frequency (RF) magnetron sputtering at a substrate temperature of 350 °C. The synthesized TiO2 nanostructures were annealed at 550 °C for 2 h and examined via X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), photoluminescence (PL), and Raman spectroscopy. The XRD patterns showed the presence of the peaks characteristic of rutile phase. The band gap of the TiO2 nanostructures was calculated using the UV–vis absorption spectrum and was determined to be between 3.15 and 3.24 eV. The Raman spectra contained three characteristic bands at 232, 446 and 612 cm−1, which correspond to the tetragonal TiO2 rutile. The results showed good quality of nanocrystalline TiO2 rutile phase.